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I've been trying to do water shots for months now and come up with nada!
Perhaps I'll try it at the shutter speed you did
You will want fairly low surrounding light so that the shutter speed does not play a part in the exposure but rather let the low power flash be the main source of light.
The problem with the D70 and the sb600 is that it limits the shutter speed when it doesnt need to. There is no way to set the shutter speed to 8000th of a second and have the nikon flash attached. The reason you need to tape the 2 pins is to stop the Nikon flash from telling the camera to limit the shutter speed. If you have a non nikon flash then you can set the shutter to 1/8000 and take the photos as I did. Hope this helps..